• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    Tea is aromatized with an aromatizing composition, in the form of a granulate or suspension, comprising one or more aroma- beta - cyclodextrin inclusion complexes, water, and a binding agent selected from dextran, soluble starch, gum acacia, methyl cellulose, linear dextrin, hydroxyethyl cellulose or mixtures of any of these. The tea is particularly adopted for use in tea bags.
    公开号:SU1382392A3
    申请号:SU813251307
    申请日:1981-02-18
    公开日:1988-03-15
    发明作者:Сейтли Йожеф；Сейтли Магдолна；Сенте Лайош
    申请人:Хиноин Дьедьсер Еш Ведьесети Термекек Дьяра (Инопредприятие)；
    IPC主号:
    专利说明:

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    The invention relates to the food industry and relates to a composition for the preparation of tea flavoring,
    The aim of the invention is to prevent the separation of tea after aromatization with the composition, or thereby stability.
    Aromatic substances can be protected from the adverse effects of the atmosphere by imprisonment in a cyclodextrin complex. The combination of the complex eliminates the volatility of the aromatic substance and protects predominantly easily oxidizable aromatic molecules from the oxidizing effect of the atmosphere.
    Tea before brewing contains an aromatic substance in the form of a cyclodextrin complex. Under the action of hot water, the aromatic substance is released from the cocktail to the milk.
    The size of the small grains of the complex is insufficient when flavoring tea with a cyclodextrin complex ..
    Although the size of the fine grains makes it easier to mix the aromatic complex with the leaves of the tea, the mixture is separated in the machine, which loads the ketics.
    The proposed composition dissolves quickly and easily in hot water and does not change the color and transparency of the tea — and, moreover, does not add any other taste or aroma to its own aroma.
    The dextran binder used according to the invention (dextrin, soluble starch, gum arabic, methylcellulose, hydroxyethylcellulose) does not affect the manufacture of tea. The binder is dissolved in hot water without affecting the color or translucency of the tea and adding a different flavor or aroma to the tea scent.
    The total amount of dextran used as a binder (and / or soluble starch, and / or gum arabic, and / or methylcellulose, and / or linear dextrin, and / or hydroxyethylcellulose) in the granulate is mainly 20- 30 weight.h. in terms of JOG weight.h. aromatic components
    Glycerin and water prevent fragility of position and processed tea. Binders can be used alone or in combination. The proposed number of each

    10 15
    20
    , 35
    40 45
    Jq
    The 55th of this component ensures the strength of the flavoring granules, which are not exfoliated during transportation and packaging. Work mainly with dextran.
    From the point of view of aesthetics, it is advantageous if the color of the granule is similar to the color of the tea leaf, so the granulate can be painted with tea leaf powder.
    In the manufacture of a granulate according to the invention from a flavoring composition, from a solid binder and, if desired, from the tea leaf powder, the mixture is prepared and glycerin and water are introduced into the kneader. After homogenization of the mixture, the resulting pasty mass is granulated, dried, milled and the fraction with a particle size of 0.5-1 mm is sifted out. Larger granules are ground again, smaller ones are replaced again with a small amount of water, granulated, dried and ground. As a result, the entire quantity of the mixture is converted into granules with the required size I
    grains. The specific volume of the granules corresponds to the specific volume of the tea leaf and the separation observed earlier is not observed upon shaking the flavored mixture. Flavored with the proposed suspension tea is also resistant. The suspension binder fixates the aromatized incorporated complexes on the tea leaves.

    As an aromatic / s-cyclodextrin-activated aromatizing complex, the preparations according to the invention contain mainly included bergamot, jasmine, lemon and anise complexes; sat down and can be replaced separately or B combinations.
    The preparation of the included complexes is carried out as follows.
    With a stirring, the volatile oil or its ethanol or ethanol or ethanol solution added to the complex is added to the heat of the aqueous-alcoholic solution of α-cyclodextrin. While cooling the reaction mixture, a crystal-like complex of the corresponding volatile oil precipitates.
    Example 1. A pasty paste is prepared in a kneader; a bulk mass is used, and 250 g of 1 included berganochiko oil complex i is used.
    cyclodextrin, 50 g of dextran (average mol.v. 43,000), 25 ml of glycerol and 25 ml of water.
    The resulting mass is granulated at room temperature and dried. The dry granulate is milled and fractionated on a sieve. The fraction with a grain size of 0.5-1 mm can be mixed with tea leaf. The fraction with a larger grain size is ground again, and the fraction. With a smaller grain size, a small amount of water is added and mixed, granulated, ground, and fractionated. As a result, the entire amount of the mixture is practically converted into a fraction with the required grain size. 330 g of granules are obtained, containing 76% by weight of a complex of bergamot oil,
    EXAMPLE 2: Perform, analogously to example 1, but 250 kg of the included bergamot oil / 5-cyclodextrin complex replace 250 g of the included jasmine oil-β-cyclodextrin complex,
     Example 3, is carried out analogously to Example 1, but 250 g of the included bergamot oil- / 3-cyclodextrin complex are replaced with 250 g of the included peppermint-A-cyclodextrin oil complex,
    PRI me R 4 Vsholnayut similar
    The flavored tea is stored in filter bags in cardboard (consequently, non-hermetically sealed) for 1 g at room temperature example of J, but 250 g of the included bergamot oil-p-cyc-, round complex. 250 g of inslodextrin carried out after this were switched on with devices and sensitive complex of lemon oil- / 5-cyclodextrin,
    PRI me R 5, performed analogously to example J, but 250 g of the included Q complex of bergamot oil- / 1-cyclodextrin is replaced with 250 g of the included complex of anise oil- / 5-cyclodextrin,
    Example A pasty mass is prepared in a ds kneader; 25 g of the included bergamot oil- / j-cyclodextrin j complex are applied; 2.5 g of dextran, 4 g of dextrin, 0.5 g of glycerin and 6 ml of water.
    The resulting mass is further processed into granules analogously to Example 1, and using the same amount of gum arabic, soluble starch, hydroxyethylcellulose, or a mixture of them instead of dextran or dextrin, you get a similar result.
    Example 7 In a kneader, a pasty mass is prepared.
    50
    55
    I perceived that by the 1st elements showed the same amount of aromatic substance and the same aromatizing effect as in the case of the fresh preparation.
    PRI me R 9, Make a suspension of 2.8 g of the included complex of jasmine oil-cyclodextrin, 0.56 g of dextran (average mol.v, 43000), 0.28 g of glycerin and 6 ml of water
    28 g tea leaves for sachets are mixed in a laboratory pelletizer and using a small atomizer, the suspension with a stream of nitrogen is sprayed onto the tea leaves. Sprayed tea leaves with air blowing are dried with constant stirring. The resulting flavored tea leaves can be used to make sachets for batch packaging using the appropriate machine.
    0
    five
    0
    15 g of included bergamot oil-L-cyclodextria complex, 15 i- tea leaf powder, 6 g dextran, 3 ml glycerol and J3 ml water.
    The resulting mass is processed as in Example J. 40 g of a dark gray granulate is obtained, containing 37.5 wt.% Of the included bergamot oil / 3-cyclodextrin complex.
    Example JOO kg of tea leaf for bags and 2 kg of the granulate prepared according to Example 2 are mixed, and the mixture is filled with a filter using the appropriate machine in filter bags 1e. 1.5 g of tea mixture is packed in each bag.
    Flavored tea is prepared in a similar way from the remaining granules. Apply the following amount of granulate in terms of 100 kg of tea leaf: 8 kg of tabergamot oil granules (made according to examples J, 6 or 7) or 20 kg of ta-lemon oil granules (made according to example 4), or 4 kg of grams - zero ta-peppermint oil (made according to example G), or 4 kg of granules of ta-anise oil (made according to example 5).
    Flavored tea is stored in filter bags in cardboard (therefore, unhermetically sealed) for 1 g at room temperature. The investigations carried out after this with instruments and sensitive
    round. The investigations carried out after this with instruments and sensitive

    I perceived that by the 1st elements showed the same amount of aromatic substance and the same aromatizing effect as in the case of the fresh preparation.
    PRI me R 9; A suspension is made of 2.8 g of the included jasmine-α-cyclodextrin complex, 0.56 g of dextran (average mol.v, 43000), 0.28 g of glycerin and 6 ml of water.
    28 g tea leaves for sachets are mixed in a laboratory pelletizer and using a small atomizer, the suspension with a stream of nitrogen is sprayed onto the tea leaves. Sprayed tea leaves with air blowing are dried with constant agitation. The resulting flavored tea leaves can be used to make tea bags for batch packaging using a suitable machine.
    Example 10. The procedure was carried out in the same manner as in Example 9, but instead of 0.56 g of dextran, 0.56 g of water-soluble starch was used to prepare a suspension. The suspension is sprayed onto the tea leaves with compressed air.
    Example 11. The procedure was carried out analogously to Example 9, but instead of 0.56 g of dextran, 0.84 g of linear dextrin was used to prepare a suspension.
    Example 12. The suspension is made from 25 g of the included complex of lemon oil- / cyclodextrin, 3 g of dextran, 3 g of linear dextrin, 0.25 g of glycerin and 44 ml of water.
    The resulting suspension is sprayed onto 250 g of tea leaves, as indicated in Example 9.
    Example 13, similar to Example 9, but instead of 2.8 g of the included jasmine-5-cyclodextrin complex is used as the aromatic component 2.0 g of the incorporated bergamot oil- /} - cyclodextrin complex or 2.2 g of included peppermint / 5 cyclodextrin oil complex, or 3.2 g
    of the anisol-cyclodextrin complex included.
    The flavored tea preparations made according to the invention are packaged in filter bags and stored in cardboard boxes.
    权利要求:
    Claims (1)
    [1]
    Invention Formula
    A composition for producing tea flavoring, comprising a complex of an aromatic substance with a / 5-cyclodextrin, characterized in that, in order to prevent the separation of tea after aromatization with the composition and thereby increase its stability,
    JOO mac.ch complex of aromatic substance with -cyclodextrin, 10-40 mas.h. dextran, 2-20 ma.ch. gly cerin, JO-iOO MA water to formulate a granulate composition
    grain size 0.5-1.0 mm or 12- 28 mas. Dextran, 1-14 mA. glycerol, 176-300 ma.ch. water in the case of production in the form of a suspension.
    类似技术:
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    JPH11127774A|1999-05-18|Production of powdered hinoki wood knot containing pine leaf powder and rhododendron leaf powder
    BE723717A|1969-04-16|
    同族专利:
    公开号 | 公开日
    PL125711B1|1983-06-30|
    FI67168C|1985-02-11|
    NO152072B|1985-04-22|
    LU83149A1|1981-06-05|
    YU37381A|1984-02-29|
    FR2484205B1|1984-04-27|
    SE450453B|1987-06-29|
    CS250245B2|1987-04-16|
    ES500423A0|1982-01-16|
    NO152072C|1985-07-31|
    GB2074838A|1981-11-11|
    ES8201406A1|1982-01-16|
    SE8101071L|1981-08-19|
    NL8100763A|1981-09-16|
    FI810446L|1981-08-19|
    CH656778A5|1986-07-31|
    FI67168B|1984-10-31|
    DK158763C|1990-12-17|
    CS250209B2|1987-04-16|
    GB2074838B|1983-11-09|
    DE3105666A1|1982-01-07|
    PL229721A1|1981-10-30|
    DK158763B|1990-07-16|
    FR2484205A1|1981-12-18|
    DD156414A5|1982-08-25|
    CA1168090A|1984-05-29|
    FR2475858B1|1985-03-29|
    NO810530L|1981-08-19|
    DK69481A|1981-08-19|
    FR2475858A1|1981-08-21|
    YU42716B|1988-12-31|
    引用文献:
    公开号 | 申请日 | 公开日 | 申请人 | 专利标题
    US3528819A|1967-02-16|1970-09-15|Cpc International Inc|Eliminating undesirable taste from coffee and tea extracts and products|
    JPS5644905B2|1973-11-26|1981-10-22|
    GB1564001A|1975-10-24|1980-04-02|Unilever Ltd|Beverge compositions|
    HU174699B|1977-07-01|1980-03-28|Chinoin Gyogyszer Es Vegyeszet|Process for preparing cyclodextrin inclusion complexes of natural and synthetic spices, aromatic and flavoring materials|NL8203963A|1982-10-14|1984-05-01|Naarden International Nv|METHOD FOR AROMATIZING DRY VEGETABLE MATERIAL|
    EP0235539B1|1986-02-05|1992-04-29|Firmenich Sa|Process for flavouring tabacco|
    DE3883273T2|1987-03-26|1994-01-27|Firmenich & Cie|Flavored food or spice.|
    US5094860A|1991-02-20|1992-03-10|Firmenich Sa|Process for the aromatization of dry vegetable matter|
    US5144964A|1991-03-14|1992-09-08|Philip Morris Incorporated|Smoking compositions containing a flavorant-release additive|
    CA2245995A1|1997-10-23|1999-04-23|Societe Des Produits Nestle S.A.|Tea bag for iced tea|
    DE69716627T2|1997-12-23|2003-07-10|Ima Spa|Device for granulating and / or coating solids|
    GB2350047B|1999-05-06|2002-07-17|Unilever Plc|Black tea manufacture|
    US6287603B1|1999-09-16|2001-09-11|Nestec S.A.|Cyclodextrin flavor delivery systems|
    AU6593701A|2000-06-30|2002-01-14|Nestle Sa|Flavouring compositions|
    GB0016312D0|2000-07-04|2000-08-23|Zylepsis Ltd|Separation method|
    US6761918B2|2002-07-18|2004-07-13|Tata Tea Ltd.|Method of processing green tea leaves to produce black tea that can be brewed in cold water|
    DE10240698A1|2002-09-04|2004-03-18|Symrise Gmbh & Co. Kg|cyclodextrin particles|
    DE102004036187A1|2004-07-26|2006-03-23|Symrise Gmbh & Co. Kg|Tea Flavoring|
    US9044049B2|2005-04-29|2015-06-02|Philip Morris Usa Inc.|Tobacco pouch product|
    AT446023T|2005-04-29|2009-11-15|Philip Morris Prod|TOBACCO BAG PRODUCT|
    US8685478B2|2005-11-21|2014-04-01|Philip Morris Usa Inc.|Flavor pouch|
    JP2009539978A|2006-06-13|2009-11-19|カーギルインコーポレイテッド|Large particle cyclodextrin inclusion complex and method for producing the same|
    US8616221B2|2007-02-28|2013-12-31|Philip Morris Usa Inc.|Oral pouch product with flavored wrapper|
    US9888712B2|2007-06-08|2018-02-13|Philip Morris Usa Inc.|Oral pouch products including a liner and tobacco beads|
    WO2009010881A2|2007-07-16|2009-01-22|Philip Morris Products S.A.|Oral pouch products with immobilized flavorant particles|
    US8119173B2|2007-07-16|2012-02-21|Philip Morris Usa Inc.|Method of flavor encapsulation through the use of a drum coater|
    US8424541B2|2007-07-16|2013-04-23|Philip Morris Usa Inc.|Tobacco-free oral flavor delivery pouch product|
    US8950408B2|2007-07-16|2015-02-10|Philip Morris Usa Inc.|Oral pouch product having soft edge|
    US8377215B2|2008-12-18|2013-02-19|Philip Morris Usa Inc.|Moist botanical pouch processing|
    US8863755B2|2009-02-27|2014-10-21|Philip Morris Usa Inc.|Controlled flavor release tobacco pouch products and methods of making|
    GB2471303A|2009-06-24|2010-12-29|Bell Flavors & Fragrances Duft Und Aroma Gmbh|Microparticles and method of making microparticles|
    US8747562B2|2009-10-09|2014-06-10|Philip Morris Usa Inc.|Tobacco-free pouched product containing flavor beads providing immediate and long lasting flavor release|
    RU2592099C2|2010-04-12|2016-07-20|Алтриа Клайент Сервисез Ллс|Packaged product with improved sealing and method|
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    US10314319B2|2013-11-20|2019-06-11|2266170 Ontario Inc.|Method and apparatus for accelerated or controlled degassing of roasted coffee|
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    法律状态:
    优先权:
    申请号 | 申请日 | 专利标题
    HU35980A|HU180557B|1980-02-18|1980-02-18|Process for improving flavour of theas|
    HU8080358A|HU180556B|1980-02-18|1980-02-18|Granules serving for aromatization of teas and method for producing same|
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